The synthesis method of tris (2,2,2-trifluoroethyl) phosphate belongs to the technical field of battery electrolyte additives. Under nitrogen protection, trifluoroethanol is used as the raw material, and acid binding agent is added to the solvent. Then, phosphorus oxychloride is added for reaction. The resulting reaction solution is filtered, washed, dried, decolorized, and concentrated to obtain tris (2,2,2-trifluoroethyl) phosphate.
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed a gas chromatograph for the determination of tris (2,2,2-trifluoroethyl) phosphate and established an analytical method for tris (2,2,2-trifluoroethyl) phosphate. The purity and impurities have been effectively separated, and the yield of the synthesized product is high, with a purity of up to 99.95%.
The vast spectrum makes the impossible possible. Establish an analysis plan based on user requirements
Name: Capillary Column
Specification: 30m * 0.32mm * 0.5um
Model: HH-TTFPa
Application: Industrial phosphoric acid tris (2,2,2-trifluoroethyl) ester - Determination of purity and impurities - Gas chromatography method
磷酸三(2,2,2‑三氟乙基)酯的合成方法，属于电池电解液添加剂的技术领域，于氮气保护下，以三氟乙醇为原料，与缚酸剂加入到溶剂中，然后加入三氯氧磷进行反应，所得反应液抽滤后，经洗涤、干燥、脱色、浓缩得到磷酸三(2,2,2‑三氟乙基)酯。
浩瀚色谱（山东）应用技术开发有限公司，研制《磷酸三(2,2,2-三氟乙基)酯测定气相色谱仪 》，，建立了磷酸三(2,2,2-三氟乙基)酯的分析方法，纯度及杂质得到有效分离，合成产物的收率高、纯度高达99.95%。
浩瀚色谱，变不可能为可能。根据用户的要求，建立分析方案
名称：毛细管柱
规格：30m*0.32mm*0.5um
型号：HH-TTFPa
应用：工业磷酸三(2,2,2-三氟乙基)酯纯度及杂质测定 气相色谱法
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